A-Base extraction by watersteam destillation

[Ferry 1 and 2]

I forgot how this works and yet all my Try outs misleaded
After the the reaction of Amalgam with the p2np IPA mixture combined with the acid, what next?
In my mind i remember something like this:

1. Put mixture in reaction flask, connect water destillation kit to it, heat it up, measure the steam temperature which slowly raises until it reaches 100% celsius, at 100 degrees celsius this means that from this point on only water is destilled with the Base in it so you start capturing the drips of liquid that come out of the destialltion unit in a cup, in the cup you put some NaOH pelltes first when you start capturing the liquid that runs out of the unit, next you get two layers in the cup from which the first layer on the ground is the destilled water and the second layer above it is the pure A-Base which then will be separated, after that you continue like the Video protocol from the Side Creator (sulfuric acid nd so on)

2. After the Amlagam reaction with the p2np IPA mixture combined with acid you put the mixture in a reaction flask, than add Water NaOH solution to the mixture and receive two layers, than heat it up and wait until 100 degrees celsius measured in the steam and so on and so on like above.

Which method is the correct way for extracting the A-Base from the reaction mixture by using water destillation process???

Or does my mind play tricks on me and I rememmber completely wrong?

How to do yo?

Thanks y'all

 

[GhostChemist]

After the reaction NaOH added to RM. The pH of the top layer should be 11-12.
Decanted the liquid layer from the precipitate
When distillation is started the first evaporated is IPA and later amine with steam

http://bbzzzsvqcrqtki6umym6itiixfhn...mine-synthesis-from-p2np-via-al-hg-video.196/

http://bbzzzsvqcrqtki6umym6itiixfhn...hydrochloride-synthesis-via-tartaric-acid.81/

 

[Ferry 1 and 2]

Bro you didn't really answer my question. I wanted to know whether option 1 or 2 is the correct way fpr water destillation cause i forgot how to do it in detail after years not being active in cooking... I also think you should add a detaailled water steam destillation video to the amphetamine forum. This is really useful for the most people here.

 

[GhostChemist]

Did you watch the video? http://bbzzzsvqcrqtki6umym6itiixfhn...hydrochloride-synthesis-via-tartaric-acid.81/

 

[amieri]

Damn , people getting demanding with the spoon feeding requests.
There was a day bee's would've gotten paranoid you were LE trying to set a hook for asking questions that the answers are somewhere.
At best might have gotten a" utfse!"

 

[Ferry 1 and 2]

nO lol BUT i DID SO NOW: i GUESS MY QUESTION GETS ANSWERED RIGHT AT THE BEGINNING OF THE VIDEO YOU QUOTED: tHE SOLUTION IS FIRRST TURNED INTO TWO LAYER WITH nAoh AND THEN the water steam destillation is started. Shuld be the same procedure for amphetamine free base water steam destillation, i got it

another question: i have serious problems getting hands on the chemicals i need. Right now i am pretty fucked casue i just can't manage to get pure Schwefelsäure as it is called in German. The acid you use for proeducing the amphetamine sulfate in the free base.

The only solution was to order 10L of that acid as 10% pureness and than cook the 10l until the 90% water are destilled off so that i receive 1L of pure Schwefelsäure at the end.

I even used ctric acid few hours ago to get at least some camphetamine itrate from it. Better than nothing at all but sucks compared to schwefelsäure method.

Can you help e with 1-2 L of schwefelsäure hig purity bro or tell me where to ask for it?