Amfetamīna sintēze no P2NP, izmantojot SnCl2 un Zn

yuiopjkl

Don't buy from me
Resident
Language
🇺🇸
Joined
Mar 14, 2022
Messages
77
Reaction score
47
Points
18
I6kJaAKTeX

Salīdzinot ar P2NP reducēšanu uz alumīnija amalgamas, šī metode nodrošina ievērojami klusāku reakciju (reakcija nav eksotermiska ), labāku iznākumu (90 %) un ļoti tīru vielu (nav nepieciešama papildu attīrīšana).

Izšķīdina 15 g P2N0 50 ml bezūdens acetona.
UwgORLNaqc
Uz magnētiskā maisītāja, kas aprīkots ar atgriezenisko dzesētāju, uzliek 100 ml kolbu ar apaļo dibenu. Pievieno acetonu un 42 g alvas(II) hlorīda dihidrāta.
WHBjLrv8Vi
Ieslēdz maisīšanu, pagaida, kamēr alvas hlorīds izšķīst, un pievieno P2NP šķīdumu acetonā.
793sHRQ2fr
Maisa 20 minūtes, temperatūra lēnām paaugstinās. Maisījuma temperatūras pazemināšanās norāda uz reakcijas beigšanos. Ielej glāzē 150 ml auksta ūdens un 4 ml 36% sālsskābes, maisījumam lēnām pievieno maisījumu maisot. Šķīduma krāsa mainās
KN9JCcf4B8
Sagatavo nātrija hidroksīda šķīdumu (200 g uz 200 ml ūdens), atdzesē līdz istabas temperatūrai un pievieno maisījumam līdz pH>10 (skābā vai neitrālā vidē oksīma ekstrakcija nav iespējama), tūlīt veidojas neorganisko sāļu nogulsnes.
MjP9Yyl5TN
Ekstrahē 3 x 50 ml eilacetāta porcijas. žāvē ar bezūdens magnija sulfātu. Uz magnētiskā maisītāja glāzē ievieto 60 ml ledus etiķskābes un pievieno iepriekš iegūto šķīdumu (oksīmu etilacetātā).
4wN1jrbhyV
Maisot pievieno 10 g cinka putekļu.
3uF8p6UE2i
Maisa 15 minūtes.
RtmbHplEDL
Pievieno atdzesētu nātrija hidroksīda šķīdumu (50 g 100 ml ūdens) līdz pH>10.

HUxwgJCtZS
Maisījumu filtrē. Pievieno 50 ml dihlormetāna, atdala organisko slāni un papildus 3 reizes ekstrahē ūdens slāni ar 20 ml DCM.
XLBWS4JoQk
Organiskos ekstraktus apvieno un žāvē virs bezūdens magnija sulfāta.
Rx4hP3e0m7

ICr7mUoQXK

Iegūstam 10 g amfetamīna bāzes šķīdumu DCM. Pievienojam 50 ml bezūdens acetona un vajadzīgo skābi, lai iegūtu attiecīgo sāli.
0uIvfkn5ty

T0sRWvYhki

NCTypHPai7
 

BlueDex

Don't buy from me
Resident
Language
🇺🇸
Joined
Dec 5, 2022
Messages
90
Reaction score
35
Points
18
Forši!
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
206
Reaction score
30
Points
28
cik ml acetona mēs šeit izmantojam
 

yuiopjkl

Don't buy from me
Resident
Language
🇺🇸
Joined
Mar 14, 2022
Messages
77
Reaction score
47
Points
18
Kamēr nav izšķīdināts viss alvas hlorīds
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
206
Reaction score
30
Points
28
Vai jums ir 37% sālsskābe?
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
206
Reaction score
30
Points
28
Vai es varu šeit lietot 37% sālsskābi nepareizi tulkots
 

yuiopjkl

Don't buy from me
Resident
Language
🇺🇸
Joined
Mar 14, 2022
Messages
77
Reaction score
47
Points
18
Es domāju, ka jā
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
206
Reaction score
30
Points
28
Tātad, vai mēs pagatavojam 200 ml ūdens un 200 g nātrija hidroksīda šķīdumu un pievienojam to šeit?
 

blacky2340

Don't buy from me
Resident
Language
🇺🇸
Joined
Sep 28, 2023
Messages
36
Reaction score
30
Points
18
Kāpēc jūs izmantojat dcm citu šķīdinātāju vietā?
 

Bigballen

Don't buy from me
Resident
Language
🇺🇸
Joined
Dec 30, 2023
Messages
5
Reaction score
3
Points
3
Es tevi mīlu
 

Bigballen

Don't buy from me
Resident
Language
🇺🇸
Joined
Dec 30, 2023
Messages
5
Reaction score
3
Points
3
Cik daudz vēlamās skābes pievienot beigās?
 

blacky2340

Don't buy from me
Resident
Language
🇺🇸
Joined
Sep 28, 2023
Messages
36
Reaction score
30
Points
18
Uzlejiet 10 ml acetona uz 1 ml koncentrētas 97%+ sērskābes 10:1 proporcijā. Ar pipeti vai šļirci lēnām piliniet šķīdumu, līdz tiek sasniegts pH 5,5. Ja tas ir pārskābināts, pievienot vairāk frībāzes, ja tas ir stipri pārskābināts un pārvēršas šķidrumā, tad uz a/b un pārkristalizēt.
 
View previous replies…

Bigballen

Don't buy from me
Resident
Language
🇺🇸
Joined
Dec 30, 2023
Messages
5
Reaction score
3
Points
3
Vai jūs zināt citus šķīdinātājus, kurus varētu izmantot DCM vietā?
 

yuiopjkl

Don't buy from me
Resident
Language
🇺🇸
Joined
Mar 14, 2022
Messages
77
Reaction score
47
Points
18
Jūs varat izmantot nepolāru šķīdinātāju (ēteri, benzolu, toluolu).
 

ActionAyi

Don't buy from me
Resident
Language
🇩🇪
Joined
Jun 20, 2023
Messages
18
Reaction score
9
Points
3
Es arī esmu domājis par toulēnu, bet man šķiet, ka blīvuma starpība ir pārāk maza, vai ne ?
 

G.Patton

Expert
Joined
Jul 5, 2021
Messages
2,825
Solutions
3
Reaction score
3,117
Points
113
Deals
1
Sveiki, paldies par ziņojumu! Tas ir patiešām interesants. 10 g amfbrīvās bāzes ir 80,4 % iznākums, diezgan labi. Cik daudz sāls jūs ieguvāt?
 

yuiopjkl

Don't buy from me
Resident
Language
🇺🇸
Joined
Mar 14, 2022
Messages
77
Reaction score
47
Points
18
Metode tika kopēta no interneta.
Es to plānoju veikt tuvākajā nākotnē.
Kad to izdarīšu, informēšu jūs.
 

Eleusius_hive_reboot

Don't buy from me
Resident
Language
🇺🇸
Joined
Oct 27, 2024
Messages
38
Reaction score
34
Points
18
i just did this synthesis successfully ! (i was very astonished, that it works, like described...!)

i used 1,7g P2NP

- created sncl2 sol. from h202 and conc HCL first, until total dissolution, quenched oxidizing agent w. Bisulfite.

- dissolved p2np in acetone / EtoH and brought solutions of sncl2/p2np-solvent together in 250ml RBF

vigourously stirred for 2hrs.

------SKIPPED OXIME ISOLATION !!!!! -----

instead gave antoher dash of conc. HCL in to the whole

and gave finely divided active-C powder a hydrogen absorber in to RM.

then three portions of Zn-dust were introduced in several heaps...with subsequent hcl/EtoH addition.

as the reagents were used up i gave a small am. of AcOH to the whole and let it further react out a 15mins.


- now i slowly alkalized to ph 12 (metal precipitates formed immediate and sank...no hassle in base extraction....did with xylene/pet.ether/naphta mixture (+a small emulsion preventing splash of 2-propanol , every extraction step...)


i pooled organic xtracts, washed them with conc.brine f. rocksalt....)

afterwards the washed org.phases were run trough fine filtering apparatus.

added a 100mls of H20 and then titrated with Hcl until ph 5,5 ~


the acidic solution was equiv. mixed with acetone / ethanol-2propanol

with concentration under stirring with surface vent.

then the pasty residue was further refined...

I OBTAINED almost 1,3g amph-hcl (hygroscopic but useable!)

so that is a fine well thought route to go, THANKS TO ORIGINAL MASTERMIND
 

Eleusius_hive_reboot

Don't buy from me
Resident
Language
🇺🇸
Joined
Oct 27, 2024
Messages
38
Reaction score
34
Points
18
* MAJOR ! update:...

I DID ONE MORE "GOD-MOVE" AFTER THIS SURPRISE RESULT:.....


I SUCCEEDED IN MODIFYING THE SYNTHESIS - AND DID A REDUCTIVE AMINATION

WITH REFINED P2P AND METHYLAMMONIUMACETATE (OR KIND OF)

IT YIELDED METHAMPHETAMINE RACEMATE.... VERY UNEXPECTED QUANTITY- QUALITY AS SAME AS THE USUAL NABH4 ROUTE I PREFERRED BEFORE...



IT WENT DOWN FROM Imine formation -[ACIDIFIED VARIANT]...... TO HYDROCHLORIDE OF SLIGHT PINK APPEARANCE OVER NIGHT !

-->AT ROOM TEMPERATURE<----

PLEASE dont be mad at me but i decided to keep specifics for myself**

it is a whole new approach to phenetylamine syntheses in general ....

CREDITS TO THIS COMMUNITY PRO INSTRUCTIONAL P2P PURIFICATION TUTORIALS / I WENT TROUGH THE HASSLE OF THE WHOLE WORKUP TECHNIQUES OF THE BB-gate wisdom ...

THE PHENYLACETONE I DERIVED BY : Fe/H+ --P2NP---> Phenyl-2-Propanone



**(exception 4 you, Patton ..i made a writeup , documenting specs etc. i think you get what these
synthesis-dynamic principles hold in value )
 

TucoSalamanca.

Don't buy from me
Resident
Language
🇹🇷
Joined
May 7, 2023
Messages
206
Reaction score
30
Points
28
Cik stundas mēs atdzesēsim nātrija hidroksīda šķīdumu?
 

yuiopjkl

Don't buy from me
Resident
Language
🇺🇸
Joined
Mar 14, 2022
Messages
77
Reaction score
47
Points
18
Kamēr tas atdziest līdz istabas temperatūrai
 
Top