Eenvoudige ruwe oplosmiddelvrije Δ8-THC synthese, vragen

[cvvvxa]

Hallo, ik kwam dit tegen op youtube en wilde het delen en vragen of iemand hier ervaring mee heeft, of verbeteringen aangezien ik van plan ben om het op grote schaal te maken. Engels is niet mijn eerste taal dus sorry voor fouten
bron :

Procedure:
CBD(25g) wordt gemengd met P-TSA(0,5g) en op een hete plaat geplaatst die is ingesteld op 120C, geroerd en verwarmd voor een uur. Daarna bevat het mengsel 75% Delta 8 THC, 2,5% Delta 9 THC, 4% CBDA, 5% exo-THC, 10% iso-THC.

Mijn belangrijkste vraag is of het rookbaar is na het wegwassen van het zuur met water en base en of Δ9 misschien geproduceerd kan worden door het te verhitten tot 70C en het daar langer te houden. Ik heb al methoden gezien om Δ9 te maken, maar dan met oplosmiddelen en dat wil ik vermijden omdat het veel moeite kost om liters tolueen kwijt te raken in vergelijking met dit. En als het mogelijk is om de rode kleur te verwijderen.

 

[William D.]

Je moet het oplosmiddel gebruiken. En andere voorwaarden met dit reagens

 

[mycelium]

There is a whole website devoted to cannabis extraction, which also includes a grip of CBD>D8 or d9.
PTSA is one way, I believe there is also a catalyst required.
I haven't been doing canna work for a few years and never did those reactions, but there are several paths that use different chemicals some make a lot of d8, some make a lot of d9, but ZERO people , and these are weed chemists a lot of them, have make d8 that does not have d9, and chromotography won't seperated them(what I read was a lot of solvent to seperated and the cost is crazy.

The d9 conversion is just as potent as distillate from weed, but it has a dif flavor(not that distillate has flavor, but yeah)

 

[mycelium]

Further more, unless you have a grip of solventless CBD, then I don't know what you would start with solventless, because you are still using poisonous shit, and none of it is organic , even if the CBD is which I doubt(I am an organic cannabis farmer, and despise shit that's not organic trying to sound healthy). Start with bulk EtOH crude, clean it dewax it filter it, recover the solvent, and crash out the CBD, super simple as cbda will crash with no effort, and then you will be starting with a pure product

 

[cvvvxa]

i did it, not that complicated but the temp and time have a lot of impact, the cleanup is pretty easy since ptsa dissolves well in water, and what do you mean by "PTSA is one way, I believe there is also a catalyst required." ptsa is the catalyst. for d9 you just do room temp in toluene, also not complicated but its painful to evaporate and wash out the toluene later, but doable, i havent played with this for a long time now

 

[mycelium]

Oh I still think it would need to be distilled in the short path, in order to purify it