lah

  1. Y

    Synthesis of Amphetamine using LAH.

    Greetings to all experienced chemists of the forum. I was thinking about a way to make amphetamine using lithium aluminum hydride in THF and phenylnitropropene. How effective is this technique? Does LAC reduce the double bond in phenylnitropropene?
  2. William D.

    Amphetamine synthesis via 1-phenyl-2-nitropropene LAH reduction

    Reagents: Lithium aluminum hydride (LAH; cas 16853-85-3) 12 g; 1,4-Dioxane 300 ml; 1-Phenyl-2-nitropropene (P2NP; cas 705-60-2) 10 g; Sodium hydroxide (25% NaOH) aq. solution; Acetone ~50 ml; Sulfuric acid ~10 ml; Equipment and glassware: Two-naked round bottom flask 1 L; Retort stand and...
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