Syntéza 1-fenyl-2-propanonu (P2P) z diethyl(fenylacetyl)malonátu

[G.Patton]

Rozumíte své otázce? Máte na mysli prostou destilaci místo vakuové? Můžete, 216 stupňů C je bod varu za normálních podmínek.

 

[kingkong84]

Can this synthesis be up scaled please

 

[G.Patton]

Hello, yes, sure

 

[Pinkbay]

Is there any other way to isolate the phenylacetic acid besides putting it in the refrigerator? Will not separating affect my future work?

 

[William D.]

You can crystallize this in a cool place and filter after. In another case, you can distill the fractions. For the following steps, you cannot leave PPA.

 

[Pinkbay]

Sir, how long does the PAA crystallization process take?