JWH-018 syntese. I lille skala.

Bigwest

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Jeg har alle ingredienserne, jeg prøver at opdele de 8 og 4 minutters bestråling på 2 og 2 minutter og lade produktet afkøle mellem dem, men det virker ikke. Kan nogen hjælpe med det pls.
 

G.Patton

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Du kan prøve at dele det op i 10-25 sek. Afkøl dem ikke for meget.
 
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Bigwest

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Hej
Jeg kontrollerede alle smeltepunkterne for mit råmateriale. Alle ting er OK. Har du prøvet denne syntese med en husstandsmikrobølgeovn?

Jeg tror ikke, det vil fungere. det kan kun gøres af en mw-reaktor
 

G.Patton

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Hej, det gjorde jeg ikke. Jeg spurgte om denne syntese for dig fra William. Tak for din feedback.
 

Bigwest

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Jeg skriver til William i pm. Jeg håber, at han vil svare. Men jeg er sikker på, at der er noget galt.
 

Nicky

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Hej... Bare en lille forklaring.
Hvor længe skal vi bestråle produktet, når vi bruger en mikrobølgeovn i hjemmet - 8-4 minutter eller 10-25 sekunder? Og skal koppen være lukket?
 

Nicky

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Bruger vi også 400w i husholdningens mikrobølgeovn?
 

41Dxflatline

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Hvis mikrobølger virker, så burde ultralyd også gøre det
 

Alex7920

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Hvilken type mikrobølgeovn er god til denne reaktion? Kan denne reaktion udføres med en mikrobølgeovn i hjemmet?
 

joejoe354354

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Hej, jeg vil gerne spørge, om denne metode ikke er egnet til masseproduktion?
 

HerrHaber

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Det kan kun lade sig gøre ved hjælp af en MW-reaktor af flowtypen, der kan opfattes som improviseret fra et husholdningsapparat, men som kræver en person med en del erfaring og nosser.
 

pakanahesa

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Hej bror, mange hilsner til dig mester. Dens lille skala til let dosis eller stærk dosis? Thx. Coz jeg prøver det 1. det er slet ikke effekt
 

William D.

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2-3 mg pr. hit. Du kan lave en reaktion i etaper, hvor hver etape kontrolleres for succes.
 

robloxgelap

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all the ingredients are easily available, but making it looks difficult. is there anyone who can help me? especially for steps 6, 7, and 8 how to filter aluminum oxide, what is the temperature for reflux, and what is the aluminum oxide filtered and then washed for? because in the next step aluminum oxide is not mentioned that it will be used again.
 

soebunies

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@robloxgelap aluminium oksida ga larut dalam etanol, suhu reflux adalah suhu titik didih pelarut, tujuan pencucian aluminium oksida agar bisa digunakan kembali di reaksi berikutnya
 
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robloxgelap

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berarti untuk membuat kembali jwh, ga perlu beli alumunium oksida lagi? dan bisa pake alumunium oksida yang sebelumnya udah pernah dipakai dan sudah di cuci?
 

soebunies

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benar, hati hati sama asep kuning yang keluar, harus selalu dipantau ya👍
 

pakanahesa

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Cek pm bro, anyway ane pake microwave rumahan itu waktu dan suhunya tetap 100 celsius atau waktunya lebih lama bro. Soalnya ga ngefek bro
 

mycelium

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I don't understand people not being able to hear EtOH in the microwave
Or maybe around here everyone has cannabis oil and makes candy and shit.
Microwaves have lights inside.
With 50ml ethanol, I hear it for 15 seconds which is normally enough to make it real warm.
Then short bursts, and looking at the beaker in the microwave.
The slightest bubbles and you stop , because it goes from a couple bubbles to over boiling almost instant.
 

William D.

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Yes, you are right. It is often necessary to stop heating, it will be gradual. But there is a solution that looks like this:
P9LmxJuQFb

The condenser is installed through the seal.
 
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