Síntesis de 1-fenil-2-propanona (P2P) a partir de dietil(fenilacetil)malonato

[G.Patton]

¿Entiende su pregunta? ¿Se refiere a la destilación simple en lugar de la de vacío? Puede, 216 grados C es el punto de ebullición en condiciones normales.

 

[kingkong84]

Can this synthesis be up scaled please

 

[G.Patton]

Hello, yes, sure

 

[Pinkbay]

Is there any other way to isolate the phenylacetic acid besides putting it in the refrigerator? Will not separating affect my future work?

 

[William D.]

You can crystallize this in a cool place and filter after. In another case, you can distill the fractions. For the following steps, you cannot leave PPA.

 

[Pinkbay]

Sir, how long does the PAA crystallization process take?