Síntesis JWH-018. A pequeña escala.

[William D.]

Cloruro de 1-naftoilo sustituido - Cloruros de 1-naftoilo 4-metoxi o 4-etilo. Cloruro de 1-amantanocarbonilo, cloruro de 2-yodobenzoilo, cloruro de 2,2,3,3-tetrametilciclopropanocarbonilo, etc.

 

[Khaled]

El sustituto del cloruro de naftoilo es el cloruro de benzoilo 99%.

 

[NarcoState]

Is this true because benzoyl chloride is obtainable when naphtoyl chloride is impossible to find.

 

[William D.]

It will be a weak substance.

 

[pakanahesa]

Is there any change of colour of reaction before and after microwave 8 mins and 4 mins? And in reflux progress the produce change colour cause of reaction?

 

[William D.]

Yes, the solution should change the color. Irradiation in small intervals of time several times.

 

[pakanahesa]

Before that the color is white, what color after irradiation?

 

[William D.]

This should become darker.

 

[pakanahesa]

If become darker how strong this formula for scale 1 to 10?

Cause i try it not even darker in irradiation 8 and 4 mins microwave cause i use home mw not mw reactor. It change color just after reflux from white form to light yellowish form