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Aluminium amalgam (Al/Hg) Summary
Ar tai gali būti naudojama sintezėms, kurioms reikia NaBH4, pakeisti? Bandau pagaminti 5-MeO-DMT iš 5-MeO-T pagal Hamiltono Norriso sintezę, tačiau neturiu prieinamo NaBH4.
- By G.Patton
Nemanau, kad taip
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ar yra būdas pasigaminti NaBH4, kuriam nereikalinga itin aukšta temperatūra ar slėgis ir kurį galima atlikti nedideliu mastu mėgėjiškoje laboratorijoje, ar tiesiog pasiduoti ir užsisakyti iš Kinijos ir tikėtis, kad muitinė manęs neapklaus?
Kodėl šiai sintezei neveikia Al/Hg. jis turėtų redukuoti iminą, kad metilinti triptaminą, ar ne?
Manau, kad tai gali būti įmanoma, bet nesu visiškai tikras. Ar manote, kad tai sumažins dvigubą indolo jungtį?
Vienintelis dalykas, dėl kurio nesu labai tikras, yra produktas, ar iš jo bus gaminamas MMT, ar DMT. Jūsų atliktoje metamfetamino sintezėje iš amfetamino su Al/Hg prie amino pridedama tik viena metilo grupė.
Kaip, paruošus gyvsidabrio tirpalą azoto rūgštyje ir įpylus šį tirpalą į kolbą su vandeniu ir aliuminio folija, tinkamai išleisti šios reakcijos dūmus? Atrodo, kad garai yra pakankamai stiprūs, todėl jie išsiskiria iš oro filtro ir prasiskverbia pro kaukę. Galvojau naudoti vakuuminį siurblį su kolba ir vakuumo reguliatorių, kad vakuumas būtų pakankamai stiprus, kad garus būtų galima išleisti į lauką, bet nerimauju dėl vandenilio dujų siurbimo, nes gali kilti sprogimo pavojus.
Sveiki, ar galiu naudoti tokį patį gyvsidabrio (Ii) chlorido kiekį kaip ir gyvsidabrio (Ii) nitrato amfetamino sintezei pls
Try doing a test run of amalgam on a small amount and you will see. It is usual to take a little more chloride than nitrate.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
But it is not always necessary that the reaction of the mercury salt be very active, many people prefer to put less mercury salt so that the reaction is calmer. It all depends on you and your conditions.
If the reaction is weak, you need more mercury salt, if it's too strong, you need less. Obviously.
I am trying to do an amalgam of 10g aluminum. I have mercuric nitrate as a liquid, 30ml,it is 1.5% mercury and I assume the rest is water. Is this enough, not enough or too much mercury for that 10g aluminum. Can the aluminum be overreacted ? Can I let the aluminum sit in the mercury solution for 24 hrs ? Like if I throw it all together and forget about it for a day till I want to use it, is it storable in the mercury solution, to stay as usable amalgam ?
Explain how you obtained 30 mL of a 1.5% solution of mercury. This is very similar to dissolving metallic mercury in nitric acid. And it's too much for 10 g of aluminum.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
If you were planning to put aluminum foil in a flask, pour in water, and add a solution of mercury nitrate, you can't store that solution. The mercury will react with the foil.
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A order from some webjoint called Zoro. It’s mercury at 1.5% , nitric acid and water. How much u think 10g aluminum will need ? 10ml ?
Either way I’ll be hawk eyeing the shit so I’ll get it done. In a week hope for good posts of good rxn or wait and see me complain for a week cuz I messed it up somehow lol
Any advice ? I’m trying this one with amalgam and I’m doing the copper synth as well
Either way I’ll be hawk eyeing the shit so I’ll get it done lol. Hope for good posts here in a week, or wait and see me complain for a week cuz I can’t do it right for some reason lol